Synthesis and Characterization of 1-phenyl-3-methyl-4-stearoylpyrazol-5-one and Its Lanthanum(III) and Tungsten(VI) Complexes

Ehirim, A. I. C. and Enenebeaku, C. K. and Asimole, C. and Ogwuegbu, M. O. C. and Ejike, E. N. O. (2020) Synthesis and Characterization of 1-phenyl-3-methyl-4-stearoylpyrazol-5-one and Its Lanthanum(III) and Tungsten(VI) Complexes. International Research Journal of Pure and Applied Chemistry, 21 (10). pp. 140-151. ISSN 2231-3443

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Abstract

The ligand, 1-phenyl-3-methyl-4-stearoylpyrazol-5-one (HSPy), and its La(III) and W(VI) complexes were synthesized and characterized spectroscopically using elemental analysis, UV-visible, IR, 1H and 13C NMR. Physical properties such as colour, melting points, conductivity measurements and solubility profile were also investigated. La(III) and W(VI) reacted with the ligand in the metal-ligand mole ratios of 1:3 and 1:2 to form neutral complexes of diaquo-trischelate La(SPy)3.2H2O and dioxoaquo-bischelate, WO2(SPy)2.H2O respectively.

Item Type: Article
Subjects: STM Library > Chemical Science
Depositing User: Managing Editor
Date Deposited: 10 Apr 2023 04:55
Last Modified: 30 Jan 2024 06:34
URI: http://open.journal4submit.com/id/eprint/1660

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