Ehirim, A. I. C. and Enenebeaku, C. K. and Asimole, C. and Ogwuegbu, M. O. C. and Ejike, E. N. O. (2020) Synthesis and Characterization of 1-phenyl-3-methyl-4-stearoylpyrazol-5-one and Its Lanthanum(III) and Tungsten(VI) Complexes. International Research Journal of Pure and Applied Chemistry, 21 (10). pp. 140-151. ISSN 2231-3443
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Abstract
The ligand, 1-phenyl-3-methyl-4-stearoylpyrazol-5-one (HSPy), and its La(III) and W(VI) complexes were synthesized and characterized spectroscopically using elemental analysis, UV-visible, IR, 1H and 13C NMR. Physical properties such as colour, melting points, conductivity measurements and solubility profile were also investigated. La(III) and W(VI) reacted with the ligand in the metal-ligand mole ratios of 1:3 and 1:2 to form neutral complexes of diaquo-trischelate La(SPy)3.2H2O and dioxoaquo-bischelate, WO2(SPy)2.H2O respectively.
Item Type: | Article |
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Subjects: | STM Library > Chemical Science |
Depositing User: | Managing Editor |
Date Deposited: | 10 Apr 2023 04:55 |
Last Modified: | 30 Jan 2024 06:34 |
URI: | http://open.journal4submit.com/id/eprint/1660 |